Buchi SpeedExtractor E-916 User Manual

Operation Manual093218 en E-916/E-914SpeedExtractor

2 Safety10 SpeedExtractor E-916/E-914 Operation Manual, Version D2.4 Safety warnings and safety signs used in this manualDANGER, WARNING, CAUTION and

10 Spare parts100 SpeedExtractor E-916/E-914 Operation Manual, Version DAccessories related to the Syncore® Analyst R-6 collection unit (only for E-9

10 Spare parts101 SpeedExtractor E-916/E-914 Operation Manual, Version DAccessories related to the extraction cellItem PU Order no.aTop cup seals for

10 Spare parts102 SpeedExtractor E-916/E-914 Operation Manual, Version DDisposablesItem PU Order no.Weighing boat 250 053202aQuartz sand, dried at 75

10 Spare parts103 SpeedExtractor E-916/E-914 Operation Manual, Version DAccessories related to the pumpItem PU Order no.ffCheck valves 1 053610Piston

10 Spare parts104 SpeedExtractor E-916/E-914 Operation Manual, Version DAccessories related with the process workflow evapo-ration to drynessItem PU O

10 Spare parts105 SpeedExtractor E-916/E-914 Operation Manual, Version DToolsItem PU Order no.a b c d e f g h i jaBit wrench 1 052783bTorx screwdrive

10 Spare parts106 SpeedExtractor E-916/E-914 Operation Manual, Version D

11 Declarations and requirements107 SpeedExtractor E-916/E-914 Operation Manual, Version D11 Declarations and requirements11.1 FCC requirements (fo

11 Declarations and requirements108 SpeedExtractor E-916/E-914 Operation Manual, Version D11.2 Declaration of conformity

2 Safety11 SpeedExtractor E-916/E-914 Operation Manual, Version DSymbol MeaningFire hazardHot item, hot surfaceDevice damageInhalation of substancesCh

BÜCHI Labortechnik AGCH-9230 Flawil 1/SwitzerlandT +41 71 394 63 63 F +41 71 394 65 65 www.buchi.com Quality in your hands

2 Safety12 SpeedExtractor E-916/E-914 Operation Manual, Version D2.5 Product safetyThe SpeedExtractor has been designed and built in accordance with

2 Safety13 SpeedExtractor E-916/E-914 Operation Manual, Version D NOTICERisk of instrument damage by liquids or mechanical shocks.• Do not spill liqu

2 Safety14 SpeedExtractor E-916/E-914 Operation Manual, Version D2.5.4 Built-in safety elements and measures• The heating element is equipped with o

2 Safety15 SpeedExtractor E-916/E-914 Operation Manual, Version D2.6 General safety rulesResponsibility of the operatorThe head of the laboratory is

2 Safety16 SpeedExtractor E-916/E-914 Operation Manual, Version D

3 Technical data17 SpeedExtractor E-916/E-914 Operation Manual, Version D3 Technical dataThis chapter introduces the reader to the SpeedExtractor an

3 Technical data18 SpeedExtractor E-916/E-914 Operation Manual, Version DList of loose partsPosition Item PU Universal Order no. E-914 Order no. E-91

3 Technical data19 SpeedExtractor E-916/E-914 Operation Manual, Version DList of loose partsPosition Item PU Universal Order no. E-914 Order no. E-91

3 Technical data20 SpeedExtractor E-916/E-914 Operation Manual, Version D3.3 Materials usedMaterials usedComponent Material designationHousing Speed

3 Technical data21 SpeedExtractor E-916/E-914 Operation Manual, Version DTechnical data of the SpeedExtractorDescription Technical dataPressure range

3 Technical data22 SpeedExtractor E-916/E-914 Operation Manual, Version D

4 Description of function23 SpeedExtractor E-916/E-914 Operation Manual, Version D4 Description of functionThis chapter explains the basic principle

4 Description of function24 SpeedExtractor E-916/E-914 Operation Manual, Version Da Main power switchThe instrument is protected by a 14 A (240 V) ci

4 Description of function25 SpeedExtractor E-916/E-914 Operation Manual, Version D4.3 Overview of the extraction processA complete extraction proces

4 Description of function26 SpeedExtractor E-916/E-914 Operation Manual, Version Dcells is absolutely mandatory. Placing the cells in the cold instru

4 Description of function27 SpeedExtractor E-916/E-914 Operation Manual, Version DabcdefghijjklmnopqrN2a Solvent reservoirs (3 and 4 optional)b Nitro

4 Description of function28 SpeedExtractor E-916/E-914 Operation Manual, Version DNOTEThe START and STOP buttons are used only for the extraction met

4 Description of function29 SpeedExtractor E-916/E-914 Operation Manual, Version Da Current extraction cycle/total extraction cyclesb Name of the cu

Table of contents3 SpeedExtractor E-916/E-914 Operation Manual, Version DTable of contents1 About this manual ...

4 Description of function30 SpeedExtractor E-916/E-914 Operation Manual, Version Dabcdea Performing a LEAK TEST (see section 6.2.5).b Flushing the l

4 Description of function31 SpeedExtractor E-916/E-914 Operation Manual, Version D4.5.3 General information on buttonsThe following control buttons

4 Description of function32 SpeedExtractor E-916/E-914 Operation Manual, Version D4.5.4 Rear connectionsabcdefa Mains supplyb Main fusec RS232 portd

5 Putting into operation33 SpeedExtractor E-916/E-914 Operation Manual, Version D5 Putting into operationThis chapter describes the installation of

5 Putting into operation34 SpeedExtractor E-916/E-914 Operation Manual, Version DNOTEThe instrument does not have to be operated under a fume hood bu

5 Putting into operation35 SpeedExtractor E-916/E-914 Operation Manual, Version D5.3 Gas and solvent connectionsN2• Connect nitrogen gas by means

5 Putting into operation36 SpeedExtractor E-916/E-914 Operation Manual, Version D5.4 DehydrationNOTEAt initial start-up or after a long period of no

6 Operation37 SpeedExtractor E-916/E-914 Operation Manual, Version D6 OperationThis chapter explains the operating elements and possible operating mo

6 Operation38 SpeedExtractor E-916/E-914 Operation Manual, Version D6.2 Preparing the instrumentThis section involves all steps required to make the

6 Operation39 SpeedExtractor E-916/E-914 Operation Manual, Version DNever use technical grade solvent. It is strongly recommended to use particle free

Table of contents4 SpeedExtractor E-916/E-914 Operation Manual, Version D6 Operation ...

6 Operation40 SpeedExtractor E-916/E-914 Operation Manual, Version DAdding a new solvent:• To add new solvents to the list go to an empty posi-tion

6 Operation41 SpeedExtractor E-916/E-914 Operation Manual, Version DSetting the preheat temperature:• Go to EXTRACTION  PREHEAT to open the preheat

6 Operation42 SpeedExtractor E-916/E-914 Operation Manual, Version DActivate all positions together:• Open EXTRACTION  OCCUPIED POSITIONS. Confirm

6 Operation43 SpeedExtractor E-916/E-914 Operation Manual, Version DMethod-based leak test Open the method:• Go to EXTRACTION  OPEN METHOD and sel

6 Operation44 SpeedExtractor E-916/E-914 Operation Manual, Version DReference setting for a standardized leak testDescription ValueTemperature 100 °CP

6 Operation45 SpeedExtractor E-916/E-914 Operation Manual, Version DIf the leak test shows that the SpeedExtractor is not tight, check the following o

6 Operation46 SpeedExtractor E-916/E-914 Operation Manual, Version Dmode when positions are deactivated. This allows a fast and efficient flushing when

6 Operation47 SpeedExtractor E-916/E-914 Operation Manual, Version D6.3 Preparing the sampleThe following sections describe all operations being invo

6 Operation48 SpeedExtractor E-916/E-914 Operation Manual, Version D6.3.2 Extraction cell selectionNOTEThe process parameters are optimized to each t

6 Operation49 SpeedExtractor E-916/E-914 Operation Manual, Version DAlternatively, use a paper or glass fiber thimble to fill in your sample. The thimbl

Table of contents5 SpeedExtractor E-916/E-914 Operation Manual, Version DRead this manual carefully before installing and running your system and note

6 Operation50 SpeedExtractor E-916/E-914 Operation Manual, Version DC Keep the sealing surfaces clean Insert the upper cellulose g (P/N 049572 for E-9

6 Operation51 SpeedExtractor E-916/E-914 Operation Manual, Version D6.4 Extraction processEach extraction procedure occurs according to a set of pred

6 Operation52 SpeedExtractor E-916/E-914 Operation Manual, Version D The heating block is fixed on movable guide rails. This allows the operator to pus

6 Operation53 SpeedExtractor E-916/E-914 Operation Manual, Version Dto 1/3 and 2/3 of the final pressure. The HEAT UP time is defined as the time during

6 Operation54 SpeedExtractor E-916/E-914 Operation Manual, Version DSpecify the vial volume:• Specification of the volume of the collection bottle is

6 Operation55 SpeedExtractor E-916/E-914 Operation Manual, Version DDefine the cycles:• Specify the number of cycles and go to the CYCLES submenu. The

6 Operation56 SpeedExtractor E-916/E-914 Operation Manual, Version DSave the method:• In order to save the modified new method, go to SAVE METHOD bac

6 Operation57 SpeedExtractor E-916/E-914 Operation Manual, Version DOperation parametersParameter Function Value range TYPE Type of solvent in solvent

6 Operation58 SpeedExtractor E-916/E-914 Operation Manual, Version D6.4.5 Example of an extraction methodExample: Extraction of 6×5 g sample in 10 mL

6 Operation59 SpeedExtractor E-916/E-914 Operation Manual, Version D6.4.7 Optimize a processThe following guidelines may help to optimize an extracti

Table of contents6 SpeedExtractor E-916/E-914 Operation Manual, Version D

6 Operation60 SpeedExtractor E-916/E-914 Operation Manual, Version D6.4.8 Start, pause, stop and abort extractionUse the green START and the red STOP

6 Operation61 SpeedExtractor E-916/E-914 Operation Manual, Version DCleaning the seals• If necessary, rinse the seals with organic solvent (e.g. etha

6 Operation62 SpeedExtractor E-916/E-914 Operation Manual, Version D

7 Maintenance63 SpeedExtractor E-916/E-914 Operation Manual, Version D7 MaintenanceThis chapter provides instructions on all required maintenance to

7 Maintenance64 SpeedExtractor E-916/E-914 Operation Manual, Version D7.2 Periodic maintenance7.2.1 Sealing systemThe condition of the cup seals is

7 Maintenance65 SpeedExtractor E-916/E-914 Operation Manual, Version DbaReplacing the lower cup seals• To replace the lower cup seals, push in the he

7 Maintenance66 SpeedExtractor E-916/E-914 Operation Manual, Version DExhaust connectionsA good indication for clogged needles or EXHAUST lines is a r

7 Maintenance67 SpeedExtractor E-916/E-914 Operation Manual, Version DabNeedlesThe needles need to be replaced regularly (i.e. at least after every 6

7 Maintenance68 SpeedExtractor E-916/E-914 Operation Manual, Version D7.3 Pump maintenancedbabeccfPump designationsa Mixer outlet lineb Pump inlet li

7 Maintenance69 SpeedExtractor E-916/E-914 Operation Manual, Version D7.3.2 Back washingBack washing is an important maintenance procedure when not o

1 About this manual7 SpeedExtractor E-916/E-914 Operation Manual, Version D1 About this manualThis manual describes the SpeedExtractor E-916/E-914 a

7 Maintenance70 SpeedExtractor E-916/E-914 Operation Manual, Version D

8 Troubleshooting71 SpeedExtractor E-916/E-914 Operation Manual, Version D8 TroubleshootingThe following chapter describes how to resume operation of

8 Troubleshooting72 SpeedExtractor E-916/E-914 Operation Manual, Version DGeneral malfunctions and their remedyMalfunction Display information Possibl

8 Troubleshooting73 SpeedExtractor E-916/E-914 Operation Manual, Version DGeneral malfunctions and their remedyMalfunction Display information Possibl

8 Troubleshooting74 SpeedExtractor E-916/E-914 Operation Manual, Version DGeneral malfunctions and their remedyMalfunction Display information Possibl

8 Troubleshooting75 SpeedExtractor E-916/E-914 Operation Manual, Version DGeneral malfunctions and their remedyMalfunction Display information Possibl

8 Troubleshooting76 SpeedExtractor E-916/E-914 Operation Manual, Version D8.1.3 Handling and resolving blockagesWhen a position gets clogged, the pre

8 Troubleshooting77 SpeedExtractor E-916/E-914 Operation Manual, Version D! CAUTIONRisk of minor or moderate injuries by hot steam of solvent when ope

8 Troubleshooting78 SpeedExtractor E-916/E-914 Operation Manual, Version DPressure >80 bar in clogged position (Errors 35-40)If the pressure in the

8 Troubleshooting79 SpeedExtractor E-916/E-914 Operation Manual, Version DMore than one position is clogged (Error 41)Once the SpeedExtractor has show

1 About this manual8 SpeedExtractor E-916/E-914 Operation Manual, Version D1.3 AbbreviationsProcess-relatedASE Accelerated Solvent ExtractionPSE P

8 Troubleshooting80 SpeedExtractor E-916/E-914 Operation Manual, Version DBlockages may be pushed out under extreme conditions. Therefore an extractio

8 Troubleshooting81 SpeedExtractor E-916/E-914 Operation Manual, Version D8.1.4 The pump is not aspirating properlyNOTEWhen the pump is running but t

8 Troubleshooting82 SpeedExtractor E-916/E-914 Operation Manual, Version D8.1.5 Replacement of check valvesThe principle of a check valve is a precis

8 Troubleshooting83 SpeedExtractor E-916/E-914 Operation Manual, Version DReplacement of sealsA damaged seal manifests itself in the form of pressure

8 Troubleshooting84 SpeedExtractor E-916/E-914 Operation Manual, Version D8.1.7 Malfunctions of the rotating valvesThe outlet and media valves are ro

8 Troubleshooting85 SpeedExtractor E-916/E-914 Operation Manual, Version D8.2 Description of the service menuThe service menu provides direct access

8 Troubleshooting86 SpeedExtractor E-916/E-914 Operation Manual, Version DDescription of the service menuService function Description Typically used f

8 Troubleshooting87 SpeedExtractor E-916/E-914 Operation Manual, Version D8.2.2 Checking the sensorsGo to SERVICE FUNCTIONS  SENSORS. The position o

8 Troubleshooting88 SpeedExtractor E-916/E-914 Operation Manual, Version D8.2.4 Inspecting the lines (flow test)Go to SERVICE FUNCTIONS  FLOW. Define

8 Troubleshooting89 SpeedExtractor E-916/E-914 Operation Manual, Version DTest 4: Heater in the back position, beaker underneath. If no pressure is bu

2 Safety9 SpeedExtractor E-916/E-914 Operation Manual, Version D2 SafetyThis chapter highlights the safety concept of the SpeedExtractor and contains

8 Troubleshooting90 SpeedExtractor E-916/E-914 Operation Manual, Version D8.2.5 Moving the cell and vial liftGo to SERVICE FUNCTIONS  LIFT. The posi

8 Troubleshooting91 SpeedExtractor E-916/E-914 Operation Manual, Version D8.3 Customer serviceOnly authorized service personnel are allowed to perfor

8 Troubleshooting92 SpeedExtractor E-916/E-914 Operation Manual, Version D

9 Shutdown, storage, transport and disposal93 SpeedExtractor E-916/E-914 Operation Manual, Version D9 Shutdown, storage, transport and disposalThis

9 Shutdown, storage, transport and disposal94 SpeedExtractor E-916/E-914 Operation Manual, Version D9.2 DisposalFor instrument disposal in an enviro

9 Shutdown, storage, transport and disposal95 SpeedExtractor E-916/E-914 Operation Manual, Version D9.3 Health and safety clearance Health and Safet

9 Shutdown, storage, transport and disposal96 SpeedExtractor E-916/E-914 Operation Manual, Version D

10 Spare parts97 SpeedExtractor E-916/E-914 Operation Manual, Version D10 Spare partsThis chapter lists spare parts and optional extras, including a

10 Spare parts98 SpeedExtractor E-916/E-914 Operation Manual, Version DAccessories related to the standard collection unitItem PU Order no.aCaps and

10 Spare parts99 SpeedExtractor E-916/E-914 Operation Manual, Version DbdcaAccessories related to the flask collection unit (only for E-914)Item PU Or