Buchi KjelFlex K-360 User Manual download pdf (Page 43)

6 Operation

43 KjelFlex K-360 Operation Manual, Version C

6.8 Carrying out a distillation

To carry out a distillation, proceed as follows:

Switch on the instrument and wait until the steam generator is ready.•

Insert the sample tube containing the sample.•

If you do not work with the titration set, prepare a conical ﬂask or a similar receptacle with a volume •

of about 250 ml as receiving vessel.

For sample analyses there are two different approaches, depending on how you prefer to work:

Single sample analyses•

Rack oriented analyses•

6.8.1 Single sample analysis

For single sample analyses, no predeﬁned sample list is needed for identiﬁcation. To start an analysis,

provide a sample and press the Sample button in the main menu. The following screen opens:

Fig. 6.14: Sample

Enter a sample name and sample weight via keypad. Choose the desired method and press Start to

start the distillation process.

NOTE

When you re-enter the screen, sample name, weight, unit, type and method are set to the latest •

entered settings.

You can start a determination at any time without a sample name or weight input.•

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Buchi KjelFlex K-360 User Manual Page 43