Buchi DuMaster D-480 User Manual

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Summary of Contents

Page 1 - Operation Manual

DuMaster D-480Operation Manual11593626 en

Page 2

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 10 Column properties (Dialog) ...

Page 3 - Copyright Note 3

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 100 Prioritizing urgent samples Via Edit > Swap you

Page 4

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 101 The following import options are available:  Imp

Page 5 - Contents

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 102 Performing other administrator tasks Target group

Page 6 - Contents 6

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 103 Modifying the registration Dialog: "Product r

Page 8 - Contents 8

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Page 9 - Contents 9

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 106 Setting up and starting up the instrument Target

Page 10 - Contents 10

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 107 Rules for first-time start-up First-time start-u

Page 11 - Contents 11

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 108  Room temperature should be constant.  Analy

Page 12

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 109 Category Type Part of initial equipment Carrier

Page 13 - General

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 11 Statistics > Clear statistic (Command) ...

Page 14 - Revision history

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 110  Filling the drying tube (on page 234).  Fil

Page 15 - About this document

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 111 Peripherals  A PC must be connected. It is ess

Page 16 - Display conventions

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 112 Detail of the rear The following picture shows a

Page 17 - Basic security settings

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 113 Removing the furnace transport protection Procee

Page 18

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 114  Push the left side door open from inside (mag

Page 19 - Warning: residual risks

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 115 CO2 intake pressure CO2 intake pressure is set a

Page 20 - Instrument casing

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 116 Shutting down the instrument Target group Person

Page 21 - Waste gas lines

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Starting up and shutting down the instrument 117 Shutting the instrument down for short measuring

Page 22 - Meaning of the warning signs

Operation Manual D-480 ©BÜCH Labortechnik AG 6 - Heating up the furnace / checking parameters 118  In case the analyzer has to be transported, m

Page 23 - Knowledge and skills

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with basic knowledge of chemistry and experience with laboratory work, e. g. ch

Page 25 - Changing mode

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 120 Measurement settings Target group Personnel with basic knowledge of chem

Page 26 - Filling reaction tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 121 Defining keywords for blank and conditioning samples Keywords Names of b

Page 27 - Filling the drying tube

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 122  Click Close to close the dialog. Required substances Different amino

Page 28

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 123 Specifying the computation method for blank value and daily factor Defin

Page 29 - Product description

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 124  ... switch off a signal, uncheck the appropriate checkbox.  Click O

Page 30 - 3 - Product description 30

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 125 Preparing samples Target group Personnel with basic knowledge of chemist

Page 31 - Technical specifications

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 126 Sample preparation instructions Samples with potential risks Various sam

Page 32 - Ambient conditions

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 127 The result will be that the nitrogen content is well measurable and you

Page 33 - Instrument design

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 128 Packing fatty, humid and non-pelletizeable solid samples - packing with

Page 34 - Front view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 129 Preparing measurement work Target group Personnel with basic knowledge o

Page 35 - Furnace section

Operation Manual D-480 ©BÜCH Labortechnik AG Purpose This chapter contains general topics of the document. In this chapter Revision history ...

Page 36 - Rear view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 130 Software usage rules Software usage rules Observe th following rules in

Page 37 - Right side view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 131  The carrier gas is reactivated and the furnaces are heated up to thei

Page 38 - Left side view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 132  Open the "Methods" dialog in the operating software by sele

Page 39 - Top view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 133 Copy methods Defining custom methods The existing method can be copied

Page 40

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 134  ... "Auto-decrement the number in the sample name": Works t

Page 41 - CHAPTER 4

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 135  This closes the dialog and the samples are swapped in the sample memo

Page 42

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 136 Performing measurement work Target group Personnel with basic knowledge

Page 43 - Functional units

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 137 Values for oxygen dosing Meaning of oxygen dosing The following illustra

Page 44 - dosing system (I)

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 138 Animal feed, approx. 500 mg medium fat content 50 mgFeed 250 ml/min, 1

Page 45

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 139 When is routine measuring work necessary? You must perform routine measu

Page 46

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 14 Revision history List of modifications in this document up to now Date Modification

Page 47

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 140  Save the data or print them out. See Data backup and printing (on pag

Page 48 - Introduction

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 141 Definitions Routine measuring work comprises the following activities: 

Page 49

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 142  Measure a maximum of 50 real samples.  At the end of the series, me

Page 50 - Setting device parameters

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 143 Checklist Go through the following list:  Were the results of a blank

Page 51 - Instrument equipment

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 144  The N integral values should be between 10 and 50 after stabilization

Page 52

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 145  Name: Blnk  Weight: 1 mg  Click Method in the line of the appropr

Page 53

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 146  Allocate the daily factor to the real samples in the sample view (tex

Page 54

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 147  Click OK. "Standard tolerance monitoring" is now enabled.

Page 55 - Calibration formulae

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 148 Preparing measuring data for evaluation Target group Personnel with basi

Page 56 - Routine measuring work

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 149 Configuring the sample view Configuring the sample view Proceed as follo

Page 57 - Daily factor determinations

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 15 About this document Status of the operating instructions The status of the operating i

Page 58 - Daily factor

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 150 Saving the sample view Saving the sample view Proceed as follows:  Ope

Page 59

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 151  You can generate statistical data manually. In this case, the user co

Page 60

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 152 Mean value The mean value of "n" element concentrations is com

Page 61 - Software user interface

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 153 Single peaks In general a single peak looks as follows: Superimposed pe

Page 62 - Sample view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 154 Manual integratability Regarding the integratability there are certain d

Page 63 - Color coding

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 155  Click and mark the peak end in the same way as described in the pre

Page 64 - Combi view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 156  The peak area was entered in the corresponding cell in the sample vie

Page 65

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 157 Setting the size of the graph with the mouse Proceed as follows:  Drag

Page 66 - Calibration view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 158 Data backup and printing Why backup and print data? The measuring data

Page 67 - Status view

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 159 Overview of export and import file formats Export and import The analysi

Page 68

Operation Manual D-480 ©BÜCH Labortechnik AG 1 - General 16 Display conventions Before you start using this guide, it is important to understand t

Page 69 - Right mouse button function

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 160  Edit the imported data as required and save them when you are finishe

Page 70 - Further functions

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 161 Working with documents Target group Personnel with basic knowledge of ch

Page 71 - Copyright Note 71

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 162 Creating new documents Usual procedure Usually, one document is created

Page 72 - Copyright Note 72

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 163 Swap samples Proceed as follows:  Open the "Swap samples" di

Page 73 - 21 CFR Part 11 functionality

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 164  A message appears which informs that the coefficients included in the

Page 74 - Versioning

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 165 Importing documents Importing documents Proceed as follows:  Open the

Page 75 - Work performed by the system

Operation Manual D-480 ©BÜCH Labortechnik AG 7 - Using the instrument 166 Checking documents for authenticity What signature is checked? Only thos

Page 76 - Requirements for operation

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Page 77 - Configure analyzer

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 168 Important information about maintenance Target group Personnel au

Page 78 - Defining logon timeout

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 169 Maintenance work to be performed by the customer Note Observe tha

Page 79 - Creating new sections

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel working with the instrument. Purpose This section describes basic safety rules

Page 80

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 170 Viewing the status of maintenance intervals Viewing maintenance i

Page 81 - LIMS export settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 171 Status view message If the maximum number of measurements is reac

Page 82

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 172 Safety instruction Strictly observe the safety instruction &quo

Page 83 - Granting authorizations

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 173  Baking out tubes to remove moisture and contaminations from th

Page 84

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 174 Safety instruction Strictly observe the safety instruction &qu

Page 85 - Defining interfaces

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 175 Performing the calibration Target group Personnel authorized by B

Page 86

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 176 Viewing list of defined factor, monitor and standard samples View

Page 87 - Dialog details

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 177 Viewing calibration coefficients Viewing calibration coefficients

Page 88 - Editing analysis data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 178 Process The section is divided into the following phases:  Prep

Page 89

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 179  Set oxygen dosing parameters (method) for conditioning and cal

Page 90 - Performing checks

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 18 Working with the operating instructions Operating the analyzer Read th

Page 91

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 180  Click OK to save your settings and close the dialog. The "

Page 92 - Viewing the logbook

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 181  If deleting has not had the desired effect, you can undo it. T

Page 93 - Working with the database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 182 Assessing the calibration curves Calibration curve display in the

Page 94 - Database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 183 The following table explains the characteristics relating to the

Page 95 - Database backup

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 184

Page 96 - Reorganize database

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 185 Calibration tables Target group Personnel authorized by BÜCHI Lab

Page 97

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 186 Calibration table for nitrogen calibration Suggestion The followi

Page 98

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 187 Replacing the ash crucible Target group Personnel authorized by B

Page 99 - Sleep/wake-up behavior

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 188 Purpose and frequency of crucible replacement Why replace the ash

Page 100

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 189 Furnace area The following picture shows the details of the furna

Page 101 - Optimizing data evaluation

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 19  Read the instructions on the individual chemicals in the safety dat

Page 102

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 190  Press the post combustion tube plug (1) and the combustion tub

Page 103 - Printer setup

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 191  Place the ash crucible in the tube rack into the vent or else

Page 104

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 192  Insert the new ash crucible into the combustion tube (4).  P

Page 105 - CHAPTER 6

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 193 Replacing sealing elements Target group Personnel authorized by B

Page 106

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 194 When to replace sealing elements What sealing elements are used?

Page 107 - General requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 195 Visual o-ring/quad ring check You can tell when o-rings or quad r

Page 108 - Specific requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 196 Ball valve maintenance Target group Personnel authorized by BÜCHI

Page 109 - Start-up

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 197 Removing and dismantling the ball valve Note The following sectio

Page 110 - Connecting peripherals

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 198 Furnace area The following picture shows the details of the furna

Page 111 - Configuring the balance

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 199 Furnace area The following picture shows the details of the furna

Page 112

ImprintProduct Identification: Operation Manual, DuMaster D-480 11593626 enBÜCHI Labortechnik AG Meierseggstrasse 40 Postfach CH-9230 Flawil 1E-Mail: q

Page 113

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 20  Contact with the substances may lead to chemical burns or poisoning

Page 114 - Default instrument settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 200 Phase 4: Dismantling the ball valve Please observe the following

Page 115 - Flow rate

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 201  Remove the ball and top half shell by means of the "knock

Page 116 - Shutting down the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 202 Process The section is divided into the following phases:  Clea

Page 117 - Procedure

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 203 Phase 2: Assembling the ball valve Proceed as follows:  Slighly

Page 118 - Safety instruction

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 204 Furnace area The following picture shows the details of the furna

Page 119 - Using the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 205 Maintaining the Ni flap and the O2 lance Target group Personnel a

Page 120 - Measurement settings

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 206 Purpose and frequency of maintaining the Ni flap and O2 lance Why

Page 121 - Viewing the list

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 207 Furnace area The following picture shows the details of the furna

Page 122

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 208 Phase 2: Removing the Ni flap (continued) Proceed as follows: 

Page 123

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 209 Installing the Ni flap Note The following section is a continuati

Page 124 - Configuring error handling

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 21  Front door  Left side door  Rear wall  Instrument cover. The

Page 125 - Preparing samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 210  Place the ungreased seal on the combustion tube connection (3)

Page 126 - Determining sample weight

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 211 Process This maintenance work is always carried out together with

Page 127 - Packing samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 212 Installing the O2 lance Proceed as follows:  Pull on the lance

Page 128

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 213 Removing, cleaning and installing the quartz glass bridge Target

Page 129 - Preparing measurement work

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 214 Removing the quartz glass bridge Process The section is divided i

Page 130 - Waking up the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 215 When to clean the quartz glass bridge The quartz glass bridge mus

Page 131 - Defining custom methods

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 216 Note: When you close a ground-in ball-and-socket joint, you must

Page 132 - Defining the Kjeldahl factor

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 217 Removing, cleaning and installing the carousel Target group Perso

Page 133 - Settings for sample input

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 218 Removing, cleaning and installing the carousel Purpose of cleanin

Page 134 - Prioritizing urgent samples

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 219  Lift off the ring at the pilots.  Clean the plastic top se

Page 135 - What can you optimize?

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 22 Warning signs on the analyzer Warning sign furnace The following pictu

Page 136 - Performing measurement work

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 220 Emptying and filling reaction tubes Target group Personnel author

Page 137 - Values for oxygen dosing

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 221 Emptying reaction tubes Requirements: Before starting work, the f

Page 138 - Performing measurements

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 222 Filling the combustion tube Note Note the following rules:  O

Page 139

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 223  Pour the recommended amounts of copper oxide (CuO) and corundu

Page 140 - Overview

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 224  Insert the wire mesh ronde.  Fill the chemicals through the

Page 141

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 225 Filling the reduction tube Proceed as follows:  Furnish both pl

Page 142 - Checklist

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 226 Removing/installing and conditioning the reaction tubes In this s

Page 143 - Background

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 227 Removing the reaction tubes from the furnace Process The section

Page 144 - Determining blank values

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 228 Top view furnace The following picture shows a top view of the fu

Page 145 - Determining the daily factor

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 229  Remove the quartz glass bridge. Hold the quartz glass bridge a

Page 146

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 23 Warning: changes to the instrument Safe instrument The analyzer is des

Page 147 - Stopping continuous analysis

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 230 Top view furnace The following picture shows a top view of the fu

Page 148

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 231 Note: When you close the ground-in ball-and-socket joints, you mu

Page 149 - Configuring the sample view

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 232  Close the front door. Phase 2: Conditioning the reaction tube,

Page 150 - Generating statistical data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 233 Filling, removing and installing the absorption and drying tubes

Page 151 - Statistical data

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 234 Filling the drying tubes Note Note the following rules:  Observ

Page 152 - Manual peak integration

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 235 Drying tube filling (large) The following picture shows the filli

Page 153 - Melted peaks

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 236 Notes regarding further operation The drying tube fillings must b

Page 154 - Integration of single peaks

Operation Manual D-480 ©BÜCH Labortechnik AG 8 - Maintaining the instrument 237 To prepare the instrument for maintenance work follow the instruc

Page 156 - Configuring the graph view

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel authorized by BÜCHI Labortechnik AG and having undergone training. Purpose This

Page 157 - Display print preview

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 24 Required personal safety equipment Protective glasses You require prot

Page 158 - Data backup and printing

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 240 Interpreting PC error messages Software reaction to errors When an e

Page 159 - Export and import

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 241 Interpreting combustion module error messages and troubleshooting Th

Page 160 - Exporting LIMS data

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 242 Performing a leak test Purpose of the leak test The leak test checks

Page 161 - Working with documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 243 Leak test procedure Process The execution of the leak test takes pla

Page 162 - Editing documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 244 F7 + F8 Furnace transformer 15 A Process The section is divided in

Page 163 - Finding documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 245 Phase 2: Remove and check fuse Proceed as follows:  If a part of t

Page 164 - Inserting data

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 246  The electrical section is now visible.  Pull out the fuse hol

Page 165 - Signing documents

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 247  Plug the protective earth conductor back into the rear wall. 

Page 166 - Checking a signature

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 248 Reacting to a power failure Open document An open document is not lo

Page 167 - Maintaining the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 249  Perform a leak test by selecting Options > Diagnostics > Le

Page 168

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 25 Damaged base panel Please observe the following instruction: Caution

Page 169 - Recommendation

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 250 Checking air-tightness of instrument Proceed as follows:  Perform

Page 170

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 251  Weigh the sample If the weight is not transmitted online, enter t

Page 171 - Installing used tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 9 - Repairing the instrument 252 Exporting analysis data Proceed as follows:  Open the "Export

Page 172 - Types of conditioning

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel involved with the instrument. Purpose This section describes the dialogs and co

Page 173 - Flushing tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 254 Dialog descriptions key Element types The following list provid

Page 174

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 255 File menu Purpose This section describes commands and dialogs f

Page 175 - Performing the calibration

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 256 File > New (Command) What is the command used for? This comm

Page 176 - Defining standard substances

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 257 Label Element type Meaning Mode Dropdown listbox Field in whi

Page 177

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 258 Label Element type Meaning Signatures Listbox column Column d

Page 178 - Requirements:

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 259 Further information Further information includes instructions i

Page 179

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 26 Removing reaction tubes Please observe the following instructions: War

Page 180

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 260 File > Delete (Command) What is the command used for? This c

Page 181

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 261 Sign (Dialog) Function In the dialog:  the user is warned abo

Page 182 - Displayed characteristics

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 262 Open You can open this dialog, if 21 CFR Part 11 functionality

Page 183 - Coefficient "a"

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 263 Label Element type Meaning Cancel Button Aborts the process an

Page 184

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 264 Open Open the dialog via: Menu command Button Hot key File >

Page 185 - Calibration tables

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 265 Print (Dialog) Function In this dialog you can define print s

Page 186 - Suggestion

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 266 Remaining elements: Label Element type Meaning OK Button Start

Page 187 - Replacing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 267 Printer setup (Dialog) Function In this dialog you can specify

Page 188 - Removing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 268 Open (Dialog) Function In this dialog you can specify the follo

Page 189 - Top view furnace

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 269 Load balance file (Dialog) Function In this dialog you can sele

Page 190

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 27 Warning Harmful substances when glass is broken! When filled quartz o

Page 191 - Installing the ash crucible

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 270 In section "Backup": Label Element type Meaning Selec

Page 192

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 271 Clean database (Dialog) Function In the dialog:  the user is

Page 193 - Replacing sealing elements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 272 Caution Data loss! Restoring the database via Restore irrevoca

Page 194

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 273 Label Element type Meaning Cancel Button Aborts the process or

Page 195 - Removing sealing elements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 274 Edit menu Purpose This section describes commands and dialogs f

Page 196 - Ball valve maintenance

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 275 Edit > Redo (Command) What is the command used for? This com

Page 197

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 276 Short cuts Invocation via the toolbar: Invocation via hot key

Page 198

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 277 Short cuts Invocation via the toolbar: Note The line to delet

Page 199 - Dismantled ball valve

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 278 If 21 CFR Part 11 functionality is enabled, a new version of th

Page 200

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 279  by clicking the right mouse key to the corresponding sample

Page 201

Operation Manual D-480 ©BÜCH Labortechnik AG 2 - Basic security settings 28 Overheating of tube fillings Please observe the following instruction:

Page 202 - Requirements

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 280 Note After invoking this command the dialog "Recalculate H

Page 203

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 281 View menu Purpose This section describes commands and dialogs f

Page 204

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 282 View > Toggle (Command) What is the command used for? This c

Page 205

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 283 Elements The following describes the elements of the dialog. La

Page 206

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 284 Elements The following describes the elements of the dialog. La

Page 207

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 285 Load views (Dialog) Function In this dialog you can reload save

Page 208

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 286 View > Gridview > Auto align (Command) What is the comman

Page 209 - Installing the Ni flap

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 287 Further information Further information includes instructions i

Page 210

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 288 Further information Further information includes instructions i

Page 211

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 289 System menu Purpose This section describes commands and dialogs

Page 212 - Installing the O

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel working with the instrument. Purpose This section provides general information

Page 213

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 290 System > Auto run (Command) What is the command used for? Th

Page 214

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 291 Note The "Abort analysis" dialog appears. Observe the

Page 215

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 292 Label Element type Meaning Cancel Button Aborts the process. F

Page 216

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 293 Label Element type Meaning Position Radiobutton Moves the car

Page 217

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 294 Further information Further information includes instructions i

Page 218 - Cleaning the carousel

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 295 Windows menu Purpose This section describes commands and dialog

Page 219

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 296 Windows > Toolbar / Run-Bar (Command) What are these command

Page 220

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 297 Icon Command Calibration > Next sample System > Wake-up

Page 221 - Emptying reaction tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 298 Label Element type Meaning No. Label Displays the number of t

Page 222 - Filling the combustion tube

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 299 Options menu Purpose This section describes commands and dialog

Page 223

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 3 Copyright © BÜCHI Labortechnik AG All rights reserved This document contains propri

Page 224 - Filling the reduction tube

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 30 Analytical characteristics and technical specifications Target group Perso

Page 225

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 300 Maintenance intervals (Dialog) Function In this dialog, any num

Page 226 - In this section

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 301 Further information Further information includes instructions i

Page 227

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 302 Commands for the maintenance of the liquid sampler VLS Commands

Page 228

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 303  Maintenance work to be performed by the customer (on page 16

Page 229

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 304 In the lower area: Label Element type Meaning Result Label Th

Page 230

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 305 Label Element type Meaning Apply Button Heats up the correspon

Page 231

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 306 Remaining elements: Label Element type Meaning Close Button Cl

Page 232

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 307 Open Open the dialog via:  Options > Diagnostics > Erro

Page 233

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 308 Label Element type Meaning autom. Auto-increment the number in

Page 234 - Filling the drying tubes

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 309 Label Element type Meaning Name Textbox/label Field to input

Page 235 - Drying tube filling (large)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 31 Analytical characteristics Analytical characteristics The following table

Page 236

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 310 Further information Further information includes instructions i

Page 237

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 311 Open Open the dialog via Options > Settings > Calculation

Page 238

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 312  If you are using multiple analyzers with one PC, you must sp

Page 239 - Repairing the instrument

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 313 In section "Network": Label Element type Meaning Path

Page 240 - Interpreting error code

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 314 Valid for all tabs: Remaining elements: Label Element type Mean

Page 241 - Performing a system test

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 315 Label Element type Meaning Peak anticipation Textbox Field to

Page 242 - Performing a leak test

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 316 Label Element type Meaning O2 dosing time Textbox Field to in

Page 243 - Replacing fuses

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 317 Elements The following describes the elements of the dialog. La

Page 244 - Fuse holder

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 318 In section "Sleep": Label Element type Meaning Sleep

Page 245

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 319 Monthly logbook (Dialog) Function This dialog contains records

Page 246 - Phase 3: Insert fuses

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 32 Interfaces USB, RS232 /V24, Safety low voltage as per DIN IEC 380/VDE 080

Page 247 - After a computer crash

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 320 Further information Further information includes instructions i

Page 248 - Reacting to a power failure

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 321 Safety instruction Strictly observe the safety instruction &q

Page 249

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 322 Entry Standard Description Parity N Defines the type of parity

Page 250

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 323 The following table describes the entries under the "Syste

Page 251 - Export for support

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 324 Label Element type Meaning OK Button Saves new settings Cancel

Page 252 - Exporting analysis data

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 325 Math menu Purpose This section describes commands and dialogs f

Page 253 - Menu and dialog descriptions

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 326 Math > Blank values > Calculate (Command) What is the com

Page 254 - Dialog descriptions key

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 327  Routine measuring work (on page 56)  Types of blank value

Page 255 - File menu

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 328 The dialog The appearance of the dialog depends on the selected

Page 256 - File > New (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 329 Elements The following describes the elements of the dialog. La

Page 257 - Listbox columns

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 33 Instrument design Target group Personnel involved with the instrument. Pur

Page 258 - Select version (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 330 Math. > Recalculate (Command) What is the command used for?

Page 259 - Save file as (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 331 Statistics menu Purpose This section describes commands and dia

Page 260 - File > Delete (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 332 Statistics > Via names (Command) What is the command used fo

Page 261 - Sign (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 333 Statistics > Include/Exclude sample (Command) What is the co

Page 262 - Export to LIMS (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 334 Calibration menu Purpose This section describes commands and di

Page 263 - Configure report (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 335 Calibration coefficients (Dialog) Function This dialog displays

Page 264 - Further information

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 336 Label Element type Meaning Cancel Button Discards calibration

Page 265 - Print (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 337 Further information Further information includes instructions i

Page 266 - Print preview (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 338 Calibration > Next sample (Command) What is the command us

Page 267 - Printer setup (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 339 Help menu Purpose This section describes commands and dialogs f

Page 268 - Open (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 34 Front view Front view, closed The following picture shows the front view o

Page 269 - Configure backup (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 340 Help > Content (Command) What is the command used for? This

Page 270

Operation Manual D-480 ©BÜCH Labortechnik AG 10 - Menu and dialog descriptions 341 In section "Analyzer": Label Element type Meaning Typ

Page 272 - Log in as (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel involved with the instrument. In this chapter Warranty ...

Page 273 - File > Exit (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 344 Warranty Target group Personnel involved with the instrument. In this section Warr

Page 274 - Edit menu

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 345 Warranty of the overall instrument Warranty of the overall instrument Please refer

Page 275 - Edit > Copy (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 346 Accessories, spare parts and consumables Target group Personnel involved with the i

Page 276 - Edit > Paste (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 347 Smallest workable unit Condition You can only order the smallest workable unit if y

Page 277 - Edit > Modify (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 348 Computer A computer is essential as the control and evaluation unit. The computer c

Page 278 - Set stop tag (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 11 - Appendix 349 Consumables set for solid samples  Optional  Required when the material from th

Page 279

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 35 Furnace section Location of the furnace section The furnace section is loc

Page 281 - View menu

Operation Manual D-480 ©BÜCH Labortechnik AG Index 351 2 21 CFR Part 11 functionality - 73, 94, 259, 260, 261, 262, 320 A About this document - 15

Page 282 - Configure view (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 352 Defining the balance / PC interface - 87 Defining the Kjeldahl factor - 132 Defining the LI

Page 283 - Column properties (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 353 Loading a sample view - 150, 285 Log in as (Dialog) - 272 M Maintaining the instrument - 16

Page 284 - Save views (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Index 354 Selecting the operating mode - 110, 131, 294 Set current weighed sample (Dialog) - 279 Set

Page 286 - Function

Technical data are subject to change without notice/Quality Systems ISO 9001.The English version is the original language version and serves as basis

Page 287

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 36 Top view furnace The following picture shows a top view of the furnace pul

Page 288 - Select columns (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 37 Right side view Right side view, closed The following picture shows the ri

Page 289 - System menu

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 38 Left side view Left side view, closed The following picture shows the left

Page 290 - System > Stop (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 3 - Product description 39 Top view Top view of the instrument The following picture shows the top vi

Page 293 - Analysis mode (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with basic chemical knowledge and basic computer knowledge. Purpose This sectio

Page 294

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 42 Layout and mode of functioning Target group

Page 295 - Windows menu

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 43 Functional units Introduction The following

Page 296 - Toolbar

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 44 I Mechanical sample insertion and O2 dosing

Page 297 - Weighing window (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 45 6 Post combustion tube with tube filling 

Page 298

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 46 Processes in the instrument during a measure

Page 299 - Options menu

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 47 Sample insertion and initiation of measureme

Page 300

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 48  Volatile halogen compounds are bound on s

Page 301 - Replace part (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 49 Basic facts about working with the instrumen

Page 302 - Leak test (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 5 Contents CHAPTER 1 General 13 Revision history ...

Page 303

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 50 Setting device parameters About instrument p

Page 304 - System test (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 51 Instrument equipment Combustion tube filling

Page 305

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 52 Filling the post combustion tube The followi

Page 306 - Error display (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 53  The daily factor for a measuring componen

Page 307 - Input options (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 54 Linear calculation over the whole range The

Page 308 - Standard samples (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 55 Polynomial calculation over the whole range

Page 309 - Keywords (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 56 Computing calibration coefficients Once the

Page 310 - Acoustic signals (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 57 Routine measuring work is performed at set i

Page 311 - LIMS settings (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 58 Blank value determination In blank value det

Page 312 - "LIMS data" tab

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 59 Understanding the operating software Target

Page 313 - "Identifier" tab:

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 6 Understanding the operating software ...

Page 314 - Device parameters (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 60 Basic functions of the operating software In

Page 315 - Method (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 61 Software user interface The main window of t

Page 316 - Error handling (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 62  ... display the online help. Details on t

Page 317

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 63 View The sample view looks like a familiar c

Page 318

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 64 Sample not yet analyzed, but a sample name

Page 319 - Monthly logbook (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 65 Progression view (graph view) Progression v

Page 320 - Select period (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 66 Statistics view The statistics view display

Page 321 - "DEVICE.INI" tab

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 67 If your series includes samples previously d

Page 322

Operation Manual D-480 ©BÜCH Labortechnik AG 4 - Understanding the instrument and planning its use 68 The areas of the status view and what they m

Page 323 - Configure key value (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 69 Copyright © BÜCHI Labortechnik AG All rights reserved This document contains propri

Page 324

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 7 Start-up ...

Page 325 - Math menu

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 70 In dialogs In dialogs you can also press the right mouse button to display certain

Page 326 - Blank values (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 71 Data administration and data security Target group Personnel with basic chemical kn

Page 327 - Define type of peak (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 72 Laboratory information and management system (LIMS) What does LIMS do? The Laborato

Page 328 - Area assignment (Dialog)

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 73 21 CFR Part 11 functionality What is 21 CFR Part 11? 21 CFR Part 11 is a regulation

Page 329

Operation Manual D-480 ©BÜCH Labortechnik AG Copyright Note 74 Restricted access to menu functions The software restricts access to the menu funct

Page 330

Operation Manual D-480 ©BÜCH Labortechnik AG Target group Personnel with good knowledge of the operating system and administrative settings. Purpos

Page 331 - Statistics menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 76 Installing and updating the software Conditions for

Page 332

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 77 Configure analyzer Target group Personnel with basi

Page 333

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 78 What can you modify in the configuration? Safety

Page 334 - Calibration menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 79 Creating new sections Safety instruction Strictly

Page 335

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 8 Setting the size of the graph ...

Page 336

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 80 Defining LIMS export settings Target group Personne

Page 337

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 81 LIMS export settings What is set? The following are

Page 338

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 82 Setting up user administration Target group Personn

Page 339 - Help menu

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 83 User administration User groups Access to menu func

Page 340 - Help > Find (Command)

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 84 Safety instruction Strictly observe the safety in

Page 341 - Short cuts

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 85 Defining interfaces Target group Personnel with goo

Page 342

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 86 Defining the analyzer / PC interface Note The opera

Page 343 - Appendix

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 87 Defining the balance / PC interface Safety instru

Page 344 - Warranty

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 88 Editing analysis data Target group Personnel with g

Page 345 - Warranty on the furnace

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 89 When does it make sense to edit analysis data? Reas

Page 346 - 11 - Appendix 346

Operation Manual D-480 ©BÜCH Labortechnik AG Contents 9 Filling, removing and installing the absorption and drying tubes ...

Page 347 - Required accessories

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 90 Performing checks Target group Personnel with good

Page 348 - Optional accessories

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 91 Checking documents for authenticity What signature

Page 349 - 11 - Appendix 349

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 92 Viewing the logbook Viewing the logbook Proceed a

Page 350

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 93 Working with the database Target group Personnel wi

Page 351 - Index 351

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 94 Database What is a database? A database is characte

Page 352 - Index 352

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 95 Defining the autoexport directory Safety instruct

Page 353 - Index 353

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 96 Autoexport Autoexport creates a backup of the curre

Page 354 - Index 354

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 97 Reorganize database Proceed as follows:  Open the

Page 355

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 98 Ways of optimizing the use of the analyzer Target g

Page 356 - Find your BUCHI Contacts:

Operation Manual D-480 ©BÜCH Labortechnik AG 5 - Work performed by the system administrator 99 Optimizing basic instrument settings Analyzer confi

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