Buchi DuMaster D-480 User Manual download pdf (Page 206)

Operation Manual D-480 ©BÜCH Labortechnik AG

8 - Maintaining the instrument 206

Purpose and frequency of maintaining the Ni flap and O2 lance

Why maintain the Ni flap and the O

lance?

Maintaining the Ni flap is necessary because the side facing to the combustion chamber will soil

which can result in an unsafe working of the Ni flap.

The O

lance will also be slightly soiled by soot which should be removed.

When to maintain the Ni flap and the O

lance?

It is recommended to check Ni flap and O

lance with each replacement of the ash crucible and clean

them if necessary.

Automatic Ni flap monitoring

Moreover, the automatic Ni flap monitoring can be enabled/disabled by the control software. As soon

as the program detects a possible contamination of the Ni flap, the analysis will be aborted and a

corresponding error message will be displayed. Further information about this topic: Error handling

(on page 316).

Removing and cleaning the Ni flap

Note

The following section describes the first part of the maintenance of the Ni flap. The topic is continued

in Installing the Ni flap (on page 209).

Process

The section is divided into the following phases:

 Preparing the instrument, gas pressure

 Removing the Ni flap

 Cleaning the Ni flap and the Ni flap flange

Safety instruction

Strictly observe the safety instruction "Hot instrument parts" under Warning notes during operation

(on page 24).

Requirements

Before starting work, the following requirements must be met:

 Keep a tube rack ready to hold hot components.

Phase 1: Preparing the instrument, gas pressure

Safety instruction

Strictly observe the safety instruction "Gas pressure" under Warning notes during operation (on

page 24).

To prepare the instrument for maintenance work follow the instructions in "Preparing the instrument:

Cool down the furnace, gas pressure" in Preparing and following up maintenance work (on page

171).

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Buchi DuMaster D-480 User Manual Page 206