Buchi Rotavapo R-220 SE User Manual Page 4
- Page / 109
- Table of contents
- TROUBLESHOOTING
- BOOKMARKS
Rated. / 5. Based on customer reviews
Table of contents
4 R-220 SE Operation Manual, Version F
5.11.2 Disinfection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
5.11.3 Sampling for determination of the germ count. . . . . . . . . . . . . . . . . . . . . 48
5.11.4 Final cleaning and drying . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
5.12 General installation instructions for glassware . . . . . . . . . . . . . . . . . . . . . 49
5.13 Single receiver. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
5.14 Heating bath filling level . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
5.15 Heating bath setup for 2×1800 W heating element . . . . . . . . . . . . . . . . . . 56
5.15.1 Water as heating transfer medium. . . . . . . . . . . . . . . . . . . . . . . . . . . 58
5.15.2 Heating transfer media with high boiling point . . . . . . . . . . . . . . . . . . . . . 59
5.16 Heating bath setup for 4.2 and 6.3 kW heating element . . . . . . . . . . . . . . . . 60
5.17 Attaching and removing evaporating flasks . . . . . . . . . . . . . . . . . . . . . . 62
5.18 Adjusting the snap flange . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
5.19 Installation and usage of a shut-off tap . . . . . . . . . . . . . . . . . . . . . . . . 65
5.20 Vacuum controller installation / removal . . . . . . . . . . . . . . . . . . . . . . . . 66
5.21 Controller upgrade . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
5.22 Final installation check. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
6 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
6.1 Evaporation in three steps. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
6.2 Optimal distillation conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
6.3 Solvent table . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
7 Maintenance and repairs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
7.1 Customer service . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
7.2 Regular service and checks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
7.2.1 System tightness . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
7.2.2 Sealings and hoses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
7.2.3 Glassware and clamps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
7.2.4 Housing, heating bath, cables and accessories . . . . . . . . . . . . . . . . . . . . 72
7.3 Snap flange coupling, flask seal and vapor duct. . . . . . . . . . . . . . . . . . . . 74
7.4 Distribution head seal and vacuum seal . . . . . . . . . . . . . . . . . . . . . . . . 77
8 Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
8.1 Resetting the over-temperature protection. . . . . . . . . . . . . . . . . . . . . . . 79
8.2 Error messages and their remedy . . . . . . . . . . . . . . . . . . . . . . . . . . . 80
8.3 Resettable automatic system fuses . . . . . . . . . . . . . . . . . . . . . . . . . . 84
9 Shutdown, storage, transport and disposal . . . . . . . . . . . . . . . . . . . . . . . . 85
9.1 Storage and transport . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
9.2 Disposal. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86
9.2.1 Lead-acid battery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86
10 Spare parts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88
10.1 Reflux glass configurations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89
10.1.1 'R' configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 90
10.1.2 'RB' configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91
10.1.3 'C' configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92
10.1.4 'BASIC' configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93
10.2 Decending glass configurations . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94
10.2.1 'D' configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
10.2.2 'D2 HP' configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96
10.2.3 'D2' configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97
10.2.4 'DB' configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98
10.2.5 'DB2' configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 99
10.3 Receiving vessel parts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .100
- Operation Manual 1
- Rotavapor 1
- R-220 SE 1
- Table of contents 3
- 1 About this manual 7
- 2 Safety 8
- SIGNAL WORD 9
- 2.5 Product safety 12
- 2.6 General safety rules 15
- 3 Technical data 16
- 3.2 Technical data 18
- Heating bath 19
- Rotational drive 19
- Glass assembly 19
- 3.3 Materials used 20
- 4 Description of function 21
- 4.2 Rotavapor front-side 23
- 4.3 Tubing scheme 24
- ** Optional accessory 29
- 12A 12A 12A 30
- (Type plate) 30
- 5 Putting into operation 33
- 5.2 Electrical connections 34
- CW Flow 37
- VAPOR TEMP 40
- CW TEMP 41
- 5.6 Condenser clamps 43
- 5.7 EasyClamps 44
- 5.8 Inlet valve 45
- 5.13 Single receiver 51
- Set Temp 56
- CW VALVE 58
- 5.21 Controller upgrade 67
- 6 Operation 68
- 6.3 Solvent table 70
- 7 Maintenance and repairs 71
- Vapor duct might slip out! 75
- 8 Troubleshooting 79
- F1 — F4 (12A, 250V) 84
- 9.1 Storage and transport 85
- 9.2 Disposal 86
- Health and Safety Clearance 87
- 10 Spare parts 88
- 10.3 Receiving vessel parts 100
- 10.4 Miscellaneous parts 101
- Part name Order no 102
- BÜCHI Labortechnik AG 109
- T +41 71 394 63 63 109
- F +41 71 394 65 65 109
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